Adducts of tungsten oxide tetrafluoride with 1,8 - naphthyridine and 2,7-dimethyl - 1,8- naphthyridine : preparation and characterization of WOF4.napy and WOF4.dmnapy
Autor: | R. Bougon, L. Arnaudet, Buu Ban, W.C. Kaska, Monique Lance |
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Rok vydání: | 1991 |
Předmět: |
Bicyclic molecule
Organic Chemistry Inorganic chemistry Infrared spectroscopy Ionic bonding Nuclear magnetic resonance spectroscopy Biochemistry Adduct Inorganic Chemistry chemistry.chemical_compound chemistry Tetrafluoride Environmental Chemistry Physical and Theoretical Chemistry Solubility Nuclear chemistry Dichloromethane |
Zdroj: | Journal of Fluorine Chemistry. 53:171-180 |
ISSN: | 0022-1139 |
DOI: | 10.1016/s0022-1139(00)82339-8 |
Popis: | The adducts WOF4.napy and WOF4.dmnapy were prepared from the reaction of WOF4 with 1,8-naphthyridine (napy) and 2,7-dimethyl-1,8-naphthyridine (dmnapy) in dichloromethane. Both adducts were characterized by elemental analysis, X-Ray powder data and infrared absorption spectroscopy. Their solubility in the usual organic solvents was found to be negligible and the trace amounts of species present in the solutions were identified as ionic derivatives originating from side-reactions. |
Databáze: | OpenAIRE |
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