Adducts of tungsten oxide tetrafluoride with 1,8 - naphthyridine and 2,7-dimethyl - 1,8- naphthyridine : preparation and characterization of WOF4.napy and WOF4.dmnapy

Autor: R. Bougon, L. Arnaudet, Buu Ban, W.C. Kaska, Monique Lance
Rok vydání: 1991
Předmět:
Zdroj: Journal of Fluorine Chemistry. 53:171-180
ISSN: 0022-1139
DOI: 10.1016/s0022-1139(00)82339-8
Popis: The adducts WOF4.napy and WOF4.dmnapy were prepared from the reaction of WOF4 with 1,8-naphthyridine (napy) and 2,7-dimethyl-1,8-naphthyridine (dmnapy) in dichloromethane. Both adducts were characterized by elemental analysis, X-Ray powder data and infrared absorption spectroscopy. Their solubility in the usual organic solvents was found to be negligible and the trace amounts of species present in the solutions were identified as ionic derivatives originating from side-reactions.
Databáze: OpenAIRE