Necílený screening organických polutantů ve vodách a sedimentech

Autor:	Hamalčíková, Veronika
Jazyk:	čeština
Rok vydání:	2011
Předmět:	extrakce kapalina-kapalina dvojrozměrná plynová chromatografie Separation methods liquid – liquid extraction sloupcová chromatografie column chromatography Separační metody mass spectrometry derivatization hmotnostní spektrometrie two-dimensional gas chromatography derivatizace
Druh dokumentu:	masterThesis
Popis:	This master thesis deals with the potential influence of the waste dump Hrádek u Pacova and the wastewater treatment plant Brno – Modřice on surroundings using the optimized non-target screening method of organic pollutants in water and sediments. The experimental part is focused on the identification of organic compounds in samples of ground water from monitoring wells, the surface water from stream and pond and in sediment samples collected from streams in the vicinity of municipal waste dump. Organic compounds were also identified in water and sediment samples from the river Svratka near the municipal waste water treatment plant Modřice. The sequential liquid – liquid extraction was used for the isolation of organic compounds in water samples. Organic compounds in sediment samples were isolated by pressurized solvent extraction (PSE) with subsequent fractionation of the extract using column chromatography. Final analysis determination was performed using comprehensive orthogonal two-dimensional gas chromatography with mass spectrometric detection (GCxGC-TOF MS).
Databáze:	Networked Digital Library of Theses & Dissertations
Externí odkaz:	http://www.nusl.cz/ntk/nusl-216788 Zobrazit plný text záznamu