SINTERING OF α-SiC WITH Y2O3-Al2O3-SiO2 GLASS ADDITIVES
Autor: | Chen-Yu Hsieh, 謝震宇 |
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Rok vydání: | 2012 |
Druh dokumentu: | 學位論文 ; thesis |
Popis: | 100 Non-reactive liquid-phase sintering of SiC has been studied using different additives. Additives were wet ball milling with SiC powder, dry-pressing at 50MPa to form disc-shaped pellets, then were sintered at 1200~15000C for 4 hours. The results indicated SiC samples with Y2O3-Al2O3-SiO2, Y2O3-Al2O3-SiO2-CaO, Ca-Al-Si-O glass additive did not show any densification after pressureless sintering. This experiment also used low melting point of Ca-Al-Si-O and Mg-B-Si-O glass as additives, and hot-pressed. The hot-pressed samples did not significantly densified either. Results indicated pressureless sintering SiC+30vol% Y2O3-Al2O3-SiO2 had the highest compressive strength of 71MPa with bulk density 1.9 g/cm3.Hot-pressed SiC+30vol% Mg-B-Si-O glass had compressive strength of 26MPa and bulk density of 2.2 g/cm3. |
Databáze: | Networked Digital Library of Theses & Dissertations |
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