Green synthesis of 2-aryl benzothiazole heterogenous catalyzed by MoO3 nanorods
| Autor: | Dighore Nitin R., Anandgaonker Priyanka, Gaikwad Suresh T., Rajbhoj Anjali S. |
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| Jazyk: | angličtina |
| Rok vydání: | 2016 |
| Předmět: | |
| Zdroj: | Green Processing and Synthesis, Vol 5, Iss 2, Pp 139-143 (2016) |
| Druh dokumentu: | article |
| ISSN: | 2191-9542 2191-9550 |
| DOI: | 10.1515/gps-2015-0065 |
| Popis: | The synthesis of MoO3 nanoparticles was done by the electrochemical method by using tetra butyl ammonium bromide (TBAB) as a stabilizer and structure directing agent in acetonitrile (ACN):tetrahydrofuran (THF) (4:1) solvent at a constant current supply of 18 mA/cm2. After heating the nanoparticles to 500°C in a muffle furnace, MoO3 nanorods were obtained. These synthesized MoO3 nanorods were characterized by UV-visible spectroscopy, Fourier transform infrared (FT-IR) spectroscopy, powder X-ray diffraction (XRD) and scanning electron microscopy. The prepared nanorods were used as heterogeneous catalysts for the synthesis of 2-aryl benzothiazole derivatives. This protocol offers several advantages such as a green method, simple work-up procedure, recyclability of the catalyst and excellent product yield in a short reaction time. |
| Databáze: | Directory of Open Access Journals |
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