Síntese da perovsquita do tipo LaNiO3 através do método dos precursores quelantes usando EDTA: otimização do teor de agente quelante

Autor: Jose Carlos dos Santos, Anne Michelle Garrido Pedrosa, Maria Eliane Mesquita, Marcelo José Barros de Souza
Jazyk: English<br />Spanish; Castilian<br />Portuguese
Rok vydání: 2011
Předmět:
Zdroj: Química Nova, Vol 34, Iss 8, Pp 1339-1342 (2011)
Druh dokumentu: article
ISSN: 1678-7064
0100-4042
DOI: 10.1590/S0100-40422011000800008
Popis: The perovskites are strategic materials due their catalytic, electronic and magnetic properties. These properties are influenced by the calcination and synthesis conditions. In this work was carried out the synthesis of LaNiO3 perovskite-type by chelating precursor method using EDTA and also was studied the optimization of the EDTA content in the synthesis. The synthesized materials were characterized by X-ray diffraction (XRD), thermal gravimetric analysis (TG) and Infrared Spectroscopy (FTIR). In the optimization of the EDTA content the lowest ratio of metal / EDTA used was 1.0 / 0.1, where it was possible to obtain monophasic perovskite.
Databáze: Directory of Open Access Journals