EFFECT OF TITANIUM SLAG PARTICLE SIZE ON THE ABILITY TO SYNTHESISE TiO₂ BY THE HYDROTHERMAL ALKALINE DISSOLUTION METHOD

Autor: Hoang Trung Ngon, Phan Dinh Tuan, Trung Kien Kieu Do
Jazyk: angličtina
Rok vydání: 2023
Předmět:
Zdroj: Ceramics-Silikáty, Vol 67, Iss 3, Pp 328-333 (2023)
Druh dokumentu: article
ISSN: 0862-5468
1804-5847
DOI: 10.13168/cs.2023.0033
Popis: Titanium slag is a by-product of iron extraction from Ilmenite ore. Titanium slag has a high TiO₂ content, so it is a suitable material for preparing TiO₂. This study investigated the influence of the slag particle size on the ability to synthesise TiO₂ by the hydrothermal alkalisation method. Three groups of titanium slag powder with average particle sizes from 18 μm to 108 μm were alkalised with a 10M NaOH solution to separate TiO₂ by the hydrothermal method. The mixing ratio by mass between the slag and the 10M NaOH solution is 1:1.5. The hydrothermal reaction was carried out at 180 °C for 7 hours. The products were analysed for their mineral, chemical, and microstructural properties using X-ray diffraction, X-ray fluorescence, scanning electron microscopy with energy-dispersive detector. The results show that the particle size significantly influences the efficiency of the TiO₂ chemical extraction from the titanium slag. The formed TiO₂ is of high purity, and the main mineral composition is anatase. The anatase polymorph of TiO₂ has the potential application as a photocatalyst and an antibacterial material.
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