Design of Experiment: A Rational and Still Unexplored Approach to Inorganic Materials’ Synthesis

Autor: Francesco Lamberti, Chiara Mazzariol, Federico Spolaore, Riccardo Ceccato, Luigi Salmaso, Silvia Gross
Jazyk: angličtina
Rok vydání: 2022
Předmět:
Zdroj: Sustainable Chemistry, Vol 3, Iss 1, Pp 114-130 (2022)
Druh dokumentu: article
ISSN: 2673-4079
DOI: 10.3390/suschem3010009
Popis: This review was devoted to outlining the use and potential increasing application of the Design of Experiment (DoE) approach to the rational and planned synthesis of inorganic nanomaterials, with a particular focus on polycrystalline nanostructures (metal and alloys, oxides, chalcogenides, halogenides, etc.) produced by sustainable wet chemistry routes based on a multi-parameter experimental landscape. After having contextualised the stringent need for a rational approach to inorganic materials’ synthesis, a concise theoretical background on DoE is provided, focusing on its statistical basis, shortly describing the different sub-methodologies, and outlining the pros and cons of each. In the second part of the review, a wider section is dedicated to the application of DoE to the rational synthesis of different kinds of chemical systems, with a specific focus on inorganic materials.
Databáze: Directory of Open Access Journals
Nepřihlášeným uživatelům se plný text nezobrazuje