High-temperature oxidation behaviour of Si3N4 nanowires with different diameters

Autor: Zhao Shuang, Yang Feiyue, Chen Jun, Li Kunfeng, Fei Zhifang, Yang Zichun
Jazyk: angličtina
Rok vydání: 2023
Předmět:
Zdroj: Processing and Application of Ceramics, Vol 17, Iss 1, Pp 39-46 (2023)
Druh dokumentu: article
ISSN: 1820-6131
2406-1034
DOI: 10.2298/PAC2301039Z
Popis: α-Si3N4 nanowires with diameters of 100-180 nm (Si3N4-W1) and 420-510 nm (Si3N4-W2) were synthesized by a modified chemical vapour deposition (CVD) method and their microstructure changes after high-temperature oxidation were studied. The results showed that both Si3N4 nanowires were not significantly oxidized when the temperature was lower than 900°C. However, the Si3N4-W1 microstructure began to change significantly after oxidation at 1200°C, while the Si3N4-W2 microstructure remained almost unchanged. Moreover, the Si3N4-W1 and Si3N4-W2 nanowires oxidized significantly after treatment at 1400°C, with weight gain of 26.4% and 13.7%, respectively.
Databáze: Directory of Open Access Journals