Autor: |
Zuhawn Sung, Arely Cano, Akshay Murthy, Daniel Bafia, Evguenia Karapetrova, Martina Martinello, Jaeyel Lee, Anna Grassellino, Alexander Romanenko |
Jazyk: |
angličtina |
Rok vydání: |
2024 |
Předmět: |
|
Zdroj: |
Scientific Reports, Vol 14, Iss 1, Pp 1-12 (2024) |
Druh dokumentu: |
article |
ISSN: |
2045-2322 |
DOI: |
10.1038/s41598-024-77905-6 |
Popis: |
Abstract Superconducting niobium serves as a key enabling material for superconducting radio frequency (SRF) technology as well as quantum computing devices. Niobium has a high propensity for the uptake of hydrogen. At room temperature, hydrogen commonly occupies tetragonal sites in the Nb lattice as the metal (M)–gas (H) phase. When the temperature is decreased, however, a solid solution of Nb-H begins to precipitate. In this study, we show the first identified topographical features associated with nanometer-size hydride phase (Nb1−xHx) precipitates on the surface of the metallic superconducting niobium using cryogenic-atomic force microscopy (AFM). Further, high energy grazing incidence X-ray diffraction reveals information regarding the structure and stoichiometry of these precipitates. Finally, through time-of-flight secondary ion mass spectroscopy (ToF-SIMS), we locate atomic hydrogen sources near the top surface. This systematic study clarifies nanometer scale hydrides precipitated on the surface of the SRF Nb cavity that exhibit performance degradation at a high accelerating field regime. |
Databáze: |
Directory of Open Access Journals |
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