Towards Real-time Control of a Semibatch Crystallization Process by Electrical and Ultrasound Tomographic Techniques

Autor: Soheil Aghajanian, Guruprasad Rao, Panagiotis Koulountzios, Lidia Jackowska-Strumillo, Manuchehr Soleimani, Tuomas Koiranen
Jazyk: angličtina
Rok vydání: 2021
Předmět:
Zdroj: Chemical Engineering Transactions, Vol 86 (2021)
Druh dokumentu: article
ISSN: 2283-9216
DOI: 10.3303/CET2186052
Popis: This research work presents a feasibility study to demonstrate the application of Electrical Resistance Tomography and transmission-based Ultrasound Computed Tomography for monitoring and control of micron-sized calcium carbonate crystallization process. Herein, precipitated calcium carbonate production is bind to a carbon dioxide absorption process based on hollow-fiber membrane contactor. ERT acquisition system is equipped with 16 electrodes with operating frequency of 156 KHz and image capturing frame rate of 2 Hz. The ultrasound tomography equipment consists of 32 piezoelectric transducers at a frequency of 200 KHz. These sensors are sensitive to changes in suspension density and conductivity. Furthermore, a process control framework is developed by utilizing the fundamental relations of settling velocity of particles. Through simulations in the LabVIEW software, the PI-based feedback controller demonstrates a possibility of setpoint tracking by manipulating the control variable (mixing speed). Upon further investigations, this approach can be used as a multi-dimensional process analytical technology tool for quality assurance and malfunction diagnosis when out-of-specification events occur throughout the entire process.
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