5-(4-Cyano-5-dicyanomethylene-2,2-dimethyl-2,5-dihydro-3-furyl)-3-(1-methyl-1,4-dihydropyridin-4-ylidene)pent-4-enyl 3,5-bis(benzyloxy)benzoate acetonitrile 0.25-solvate: a synchrotron radiation study
| Autor: | Andrew J. Kay, M. Delower H. Bhuiyan, Graeme J. Gainsford |
|---|---|
| Jazyk: | angličtina |
| Rok vydání: | 2009 |
| Předmět: | |
| Zdroj: | Acta Crystallographica Section E, Vol 65, Iss 12, Pp o3261-o3262 (2009) |
| Druh dokumentu: | article |
| ISSN: | 16005368 1600-5368 |
| DOI: | 10.1107/S1600536809050430 |
| Popis: | The title compound, C42H36N4O5·0.25CH3CN, crystallizes with a partial twofold disordered (1/4) acetonitrile solvent of crystallization. The linking atoms to the 3,5-bis(benzyloxy)benzoic acid are disordered between two conformations in the ratio 0.780 (6):0.220 (6). In the crystal, the molecules pack using mainly C—H...N(cyano) interactions coupled with weak C—H...O(ether) interactions and C—H...π interactions. A brief comparison is made between a conventional and this synchrotron data collection. |
| Databáze: | Directory of Open Access Journals |
| Externí odkaz: |
|