Probing the Use of Silane-Grafted Fumed Silica Nanoparticles to Produce Stable Transformer Oil-Based Nanofluids
Autor: | Muhammad I. Qureshi, Basit Qureshi |
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Jazyk: | angličtina |
Rok vydání: | 2021 |
Předmět: |
fumed nano-silica
plasma synthesis surface modification dispersibility plasma reactor Weibull statistical analysis Technology Electrical engineering. Electronics. Nuclear engineering TK1-9971 Engineering (General). Civil engineering (General) TA1-2040 Microscopy QH201-278.5 Descriptive and experimental mechanics QC120-168.85 |
Zdroj: | Materials, Vol 14, Iss 24, p 7649 (2021) |
Druh dokumentu: | article |
ISSN: | 1996-1944 |
DOI: | 10.3390/ma14247649 |
Popis: | In this experimental investigation, hydrophobic silane-grafted fumed nano-silica was employed in transformer oil to formulate nanofluids (NFs). A cold-air atmosphere-pressure plasma reactor working on the principle of dielectric barrier discharge was designed and utilized to functionalize the surface of these nanoparticles. A field emission scanning electron microscope (FE-SEM) coupled with energy-dispersive X-ray (EDX) module and Fourier transform infrared (FTIR) spectroscopy were used to scan surface features of new and plasma-treated nanoparticles. The study revealed considerable changes in the surface chemistry of nanoparticles, which led to good dispersibility and stability of nanofluids. The measurements of AC breakdown voltages (AC-BDV) of nanofluids so prepared were conducted according to IEC-Std 60156, and a significant improvement in the dielectric strength was achieved. A statistical analysis of these results was performed using Weibull probabilistic law. At a 5% probability of failure, modified nanofluid remarkably exhibited a 60% increase in breakdown voltage. The dielectric properties such as variation of εr and tan δ in temperature of up to 70 °C were measured and compared with untreated fluid. Results exhibit an increase in tan δ and a slight decrease in permittivity of nanofluids. The analysis also revealed that while unpolar silane coating of NPs increased the breakdown strength, the polar-amino-silane-coated NPs in oil resulted in a drastic reduction. Details of this antagonistic trend are elaborated in this paper. |
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