Determination of 17 aldehydes in Baijiu (Chinese liquor) by direct injection gas chromatography

Autor: LUO Yue, ZHONG Ciping, HUANG Ping, CHEN Yanmei, TANG Jing, YU Xiaoqin
Jazyk: English<br />Chinese
Rok vydání: 2023
Předmět:
Zdroj: Shipin yu jixie, Vol 39, Iss 10, Pp 62-68 (2023)
Druh dokumentu: article
ISSN: 1003-5788
DOI: 10.13652/j.spjx.1003.5788.2023.80024
Popis: Objective: To explore the content of aldehydes in Baijiu. Methods: A method for the determination of 17 aldehydes in Baijiu was established, and the methodological performance indexes were studied using statistics. Results: Through statistical analysis, the detection limit of 17 aldehydes in Baijiu was determined to be 0.7~5.9 mg/L, the limit of quantification was 1.9~14.6 mg/L, which passes the quality inspection of the calibration curve within the range of 0.6~320.0 mg/L, and the linear relationship meets the requirements. The recovery rate of intermediate standard addition in Baijiu was 73%~114%, the coefficient of variation in the laboratory was ≤11%, and the accuracy deviation range was -18.7%~8.0%. Conclusion: The method can be used for the determination of various aldehydes in Baijiu.
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