Efecto de la temperatura de calcinación sobre la concentración de grupos silanoles en superficies de SiO2 (SBA–15)

Autor: Reyna Ojeda-López, Isaac J. Pérez-Hermosillo, J. Marcos Esparza-Schulz, Armando Domínguez-Ortiz
Jazyk: English<br />Spanish; Castilian
Rok vydání: 2014
Předmět:
Zdroj: Avances en Química, Vol 9, Iss 1, Pp 21-28 (2014)
Druh dokumentu: article
ISSN: 1856-5301
Popis: The preparation of SBA-15 materials involves both, calcination and activation processes. The effects of the temperatures of these stages on the silanol superficial concentration are studied experimentally. The characterization techniques employed were: nitrogen adsorption, infrared spectroscopy, nuclear magnetic resonance, and X-ray diffraction. To improve the concentration of silanols groups on the solid surface, the obtained results indicate that the best temperatures of calcination and activation are 623K and 373K, respectively.
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