Qualitative TLC determination of some polycyclic aromatic hydrocarbons in sugar-beet
Autor: | Lončar Eva S., Kolarov Ljiljana A., Malbaša Radomir V., Škrbić Biljana D. |
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Jazyk: | angličtina |
Rok vydání: | 2005 |
Předmět: | |
Zdroj: | Journal of the Serbian Chemical Society, Vol 70, Iss 10, Pp 1237-1242 (2005) |
Druh dokumentu: | article |
ISSN: | 0352-5139 1820-7421 |
DOI: | 10.2298/JSC0510237L |
Popis: | The presence of polycyclic or polynuclear aromatic hydrocarbons (PAHs) were investigated in sugar-beet from a local sugar factory in the district of Vojvodina. The sugar-beet was cultivated on areas near roads with intensive traffic. The procedure for the preparation and determination of these compounds included saponification of the sample, several liquid–liquid extraction systems and a silica gel column clean-up. The purified sample solution was analysed by thin layer chromatography (TLC) on silica gel with cyclohexane as the developing solvent. Benzo(b)fluoranthene and benzo(a)anthracene and/or benzo(a)pyrene were detected at concentrations greater than the allowed limits in food. |
Databáze: | Directory of Open Access Journals |
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