Citric acid supported on melamine-based COP [CA@MIP] in metal-free on-water synthesis of quinazolinones

Autor: Atif Mustafa, Zeba N. Siddiqui
Jazyk: angličtina
Rok vydání: 2023
Předmět:
Zdroj: Tetrahedron Green Chem, Vol 1, Iss , Pp 100002- (2023)
Druh dokumentu: article
ISSN: 2773-2231
DOI: 10.1016/j.tgchem.2023.100002
Popis: A metal-free, efficient, and eco-friendly on-water protocol for the synthesis of quinazolinone derivatives via a tandem one-pot three-component reaction using a novel, efficient, and recyclable heterogeneous catalyst, [CA@MIP] – melamine-based covalent organic polymer supported citric acid, has been described. The catalyst has been synthesized by a simple procedure and is well characterized by numerous spectroscopic techniques such as Fourier Transform Infrared (FTIR), Scanning Electron Microscope (SEM), Powder X-ray diffraction (PXRD), Brunauer-Emmett-Teller (BET), Energy Dispersive X-ray (EDX), and Thermal Gravimetric (TG) analyses. [CA@MIP] showed excellent catalytic potential offering quinazolinones in excellent yields (>85%) in a short reaction time period and was reusable for up to five successive runs.
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