Autor: |
Li Xiaoyang, Zhang Genwang, Wang Binwei, Lin Tan, Wang Guo, Feng Huixia |
Jazyk: |
English<br />French |
Rok vydání: |
2019 |
Předmět: |
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Zdroj: |
E3S Web of Conferences, Vol 118, p 01059 (2019) |
Druh dokumentu: |
article |
ISSN: |
2267-1242 |
DOI: |
10.1051/e3sconf/201911801059 |
Popis: |
One-pot synthesis of polyaniline/Fe3O4 nanocomposite in 1-methyl-3-alkylcarboxylic acid imidazolium chloride ([CMMIm]Cl) ionic liquid (IL) was introduced for the first time in this work. Transmission electron microscopy (TEM), X-ray diffraction (XRD), four probes method and vibrating sample magnetometer (VSM) were used to explore the influence of IL on the structure, conductivity and magnetic properties of polyaniline/Fe3O4 composite. Compared with Fe3O4 particles prepared in water, the results show that Fe3O4 particles prepare in imidazolium-based ionic liquid were more regular in shape and dispersed uniformly. So the Fe3O4 nanoparticles prepared in IL can easier serve as cores to form the polyaniline/Fe3O4 nanocomposite via in situ chemical oxidative polymerization of aniline molecule. The saturation magnetization of polyaniline/Fe3O4 nanocomposite prepared in ionic liquid shows about 2 times higher than polyaniline/Fe3O4 composite prepared in water. And the conductivities of PANI/Fe3O4 composite prepared in IL decreased and the saturated magnetization increased with the increasing amount of Fe3O4. |
Databáze: |
Directory of Open Access Journals |
Externí odkaz: |
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