Intercalated Intermetallic Compounds AlTi3 and Fe2Ti in Microrods and Microtubes Obtained by Invariant Reaction of Mechanically Milled System Al43Ti36Fe21

Autor:	Lucía G. Díaz Barriga Arceo, Leonardo González Reyes, Jesús Noé Rivera Olvera, Abraham Medina Ovando, Vicente Garibay Febles
Jazyk:	angličtina
Rok vydání:	2019
Předmět:	mechanical alloying decomposition invariant reaction rods tubes nanostructures Technology Electrical engineering. Electronics. Nuclear engineering TK1-9971 Engineering (General). Civil engineering (General) TA1-2040 Microscopy QH201-278.5 Descriptive and experimental mechanics QC120-168.85
Zdroj:	Materials, Vol 12, Iss 23, p 3806 (2019)
Druh dokumentu:	article
ISSN:	1996-1944
DOI:	10.3390/ma12233806
Popis:	This paper reports the production of intermetallic microrods and microtubes from the decomposition of an intermetallic compound in an AlTiFe system. The intermetallic compound was obtained by mechanosynthesis of elemental powders of Al, Ti and Fe over 300 h at 400 rpm, sintering from compacted powder particles at 300 MPa per minute and at 900 °C for 3600 s in an argon atmosphere. The milled and sintered samples were analyzed by X-ray diffraction (XRD), scanning electron microscopy (SEM) and high-resolution transmission electron microscopy (HRTEM). The intermetallic AlTi3 and Fe3Al phases were obtained during the milling process. After sintering, a decomposition of these intermetallic phases was found—Al3Ti0.75Fe0.25, Al3Ti, FeTi, AlTi3, Ti9Al23, Fe2Ti, Al86Fe14 and Al0.4Fe0.6. As a result of the decomposition, we observed the formation of hexagonal rods with intercalated phases of AlTi3 and Fe2Ti.
Databáze:	Directory of Open Access Journals
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