Reaction Screening Using a Microreactor

Autor: Olivier Naef, Mathieu Roch, Thierry Chappuis
Jazyk: German<br />English<br />French
Rok vydání: 2010
Předmět:
Zdroj: CHIMIA, Vol 64, Iss 12 (2010)
Druh dokumentu: article
ISSN: 0009-4293
2673-2424
DOI: 10.2533/chimia.2010.889
Popis: This article discusses the screening of chemical reactions using a microreactor equipped with infrared spectroscopy as online analytics. An esterification reaction has been optimized in continuous mode with the proposed setup. The esterification did not work well due to the material of the microreactor (stainless-steel 316Ti) that catalyzed the decomposition of formic acid. However, despite the occurrence of decomposition, an optimization could be achieved with this system.
Databáze: Directory of Open Access Journals