Reaction Screening Using a Microreactor
Autor: | Olivier Naef, Mathieu Roch, Thierry Chappuis |
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Jazyk: | German<br />English<br />French |
Rok vydání: | 2010 |
Předmět: | |
Zdroj: | CHIMIA, Vol 64, Iss 12 (2010) |
Druh dokumentu: | article |
ISSN: | 0009-4293 2673-2424 |
DOI: | 10.2533/chimia.2010.889 |
Popis: | This article discusses the screening of chemical reactions using a microreactor equipped with infrared spectroscopy as online analytics. An esterification reaction has been optimized in continuous mode with the proposed setup. The esterification did not work well due to the material of the microreactor (stainless-steel 316Ti) that catalyzed the decomposition of formic acid. However, despite the occurrence of decomposition, an optimization could be achieved with this system. |
Databáze: | Directory of Open Access Journals |
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