Utilizing Pometia Pinnata leaf extract in microwave synthesis of ZnO nanoparticles: Investigation into photocatalytic properties
Autor: | Ari Sulistyo Rini, Yolanda Rati, Gema Maheta, Arie Purnomo Aji, Saktioto |
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Jazyk: | angličtina |
Rok vydání: | 2024 |
Předmět: | |
Zdroj: | Communications in Science and Technology, Vol 9, Iss 1, Pp 94-99 (2024) |
Druh dokumentu: | article |
ISSN: | 2502-9258 2502-9266 |
DOI: | 10.21924/cst.9.1.2024.1407 |
Popis: | In this work, ZnO photocatalyst has been synthesized using matoa (Pometia pinnata) leaf extract under various microwave irradiation powers at 360, 540, and 720 Watts for 3 minutes on each. The UV-Vis absorption spectra of ZnO exhibited a peak in the ultraviolet region 300-360 nm. UV-Vis absorption analysis revealed a decrease in the band gap energy from 3.15 eV to 3.10 eV as the irradiation power increased. Field emission scanning electron microscopy (FESEM) images displayed spherical and nanoplatelet morphology with a decrease in particle size observed from 773 to 709 nm with increasing irradiation power. X-ray diffraction (XRD) analysis confirmed the hexagonal wurtzite structure of ZnO with crystallite sizes in the range of ~18-20 nm. The synthesized ZnO nanoparticles was successfully employed as a photocatalyst in 4-nitrophenol degradation, achieving the highest degradation percentage of 82.7% at 540 Watts with a corresponding reaction rate constant of 0.0126/min. In conclusion, the microwave-assisted synthesis of ZnO using on matoa leaf extract demonstrated significant potential for the degradation of organic pollutants, thereby contributing to water purification efforts. |
Databáze: | Directory of Open Access Journals |
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