Effect of the Processing Parameters on the Porosity and Mechanical Behavior of Titanium Samples with Bimodal Microstructure Produced via Hot Pressing
Autor: | Ricardo Chávez-Vásconez, Sheila Lascano, Sergio Sauceda, Mauricio Reyes-Valenzuela, Christopher Salvo, Ramalinga Viswanathan Mangalaraja, Francisco José Gotor, Cristina Arévalo, Yadir Torres |
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Jazyk: | angličtina |
Rok vydání: | 2021 |
Předmět: |
porous titanium
bimodal microstructure hot-pressing powder metallurgy mechanical milling mechanical behavior Technology Electrical engineering. Electronics. Nuclear engineering TK1-9971 Engineering (General). Civil engineering (General) TA1-2040 Microscopy QH201-278.5 Descriptive and experimental mechanics QC120-168.85 |
Zdroj: | Materials, Vol 15, Iss 1, p 136 (2021) |
Druh dokumentu: | article |
ISSN: | 1996-1944 |
DOI: | 10.3390/ma15010136 |
Popis: | Commercially pure (c.p.) titanium grade IV with a bimodal microstructure is a promising material for biomedical implants. The influence of the processing parameters on the physical, microstructural, and mechanical properties was investigated. The bimodal microstructure was achieved from the blends of powder particles with different sizes, while the porous structure was obtained using the space-holder technique (50 vol.% of ammonium bicarbonate). Mechanically milled powders (10 and 20 h) were mixed in 50 wt.% or 75 wt.% with c.p. titanium. Four different mixtures of powders were precompacted via uniaxial cold pressing at 400 MPa. Then, the specimens were sintered at 750 °C via hot pressing in an argon gas atmosphere. The presence of a bimodal microstructure, comprised of small-grain regions separated by coarse-grain ones, was confirmed by optical and scanning electron microscopies. The samples with a bimodal microstructure exhibited an increase in the porosity compared with the commercially available pure Ti. In addition, the hardness was increased while the Young’s modulus was decreased in the specimens with 75 wt.% of the milled powders (20 h). |
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