A Facile and Catalyst-free Synthesis of Hexahydroacridine-1,8(2H,5H )-dione and Octahydroacridin-10(1H )-yl)thiourea Derivatives: Inter- and Intramolecular Aza-Michael addition

Autor:	Pesyan Nader Noroozi, Akhteh Narmin, Batmani Hana, Anıl Barış, Şahin Ertan
Jazyk:	angličtina
Rok vydání:	2020
Předmět:	cyclohexanedione octahydro-1h-xanthene acridine x-ray 1d-polymeric h-bond Organic chemistry QD241-441
Zdroj:	Heterocyclic Communications, Vol 26, Iss 1, Pp 26-32 (2020)
Druh dokumentu:	article
ISSN:	2191-0197 2020-0005
DOI:	10.1515/hc-2020-0005
Popis:	An easy and convenient technique for the one-pot synthesis of novel compounds of hexahydroacridine-1,8(2H,5H)-dione and octahydroacridin-10(1H)-yl) thiourea derivatives has been developed by the reaction of the octahydro-1H-xanthenes with hydroxylamine hydrochloride and thiosemicarbazide in ethylene glycol, which is a green solvent, under mild reaction conditions. IR, 1H NMR, 13C NMR spectrometry, and X-ray diffraction analysis were used to identify the structures of these compounds.
Databáze:	Directory of Open Access Journals
Externí odkaz:	https://doaj.org/article/6aae2406f0884c1faee06c2a9b0d4801 Zobrazit plný text záznamu View record in DOAJ