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The article presents the results of studying non-metallic inclusions (NI) after extra-furnace treatment of the 13Cr9Mo2Co1NiVNbNB steel melt to produce large-sized ingots. The objects of the study were laboratory samples (the first batch), and samples obtained after melting in industrial furnace, followed by modification and double vacuuming (the second batch). Previously, using the Fact Sage software, modeling of the NI formation processes was carried out. The data were obtained on the possible NI composition and amount in this steel. The composition, the contamination index, parameters of NI in samples have been studied. It was established that in the samples of the first batch, the main part of the NI consisted of chromium- and manganese-containing oxides, which occupy more than 94% of the total area of the NI. In the samples of the second batch, the main part of the NI was represented by aluminum containing systems. It was shown that the average size of NI in the samples after extra-furnace treatment differs slightly (5%–12%), however, the contamination index in industrial samples after vacuum treatment and especially after modification and repeated vacuum treatment was reduced by more than 10 times. The results obtained allow to recommend vacuum treatment and complex modification with calcium and boron as measures to prevent the formation of NI and to improve metallurgical quality when smelting large ingots using complex alloy steels. |
