Straightforward synthesis of 2,2,4,4,5,7,7-d7-cholestane: a new deuterated standard in petroleum analysis

Autor:	Maicon Guerra de Miranda, Andre Luis Mazzei Albert, Jari Nobrega Cardoso, Rosangela Sabbatini Capella Lopes, Claudio Cerqueira Lopes
Jazyk:	English<br />Spanish; Castilian<br />Portuguese
Rok vydání:	2013
Předmět:	total synthesis steroids deuterated standard Chemistry QD1-999
Zdroj:	Química Nova, Vol 36, Iss 8, Pp 1160-1163 (2013)
Druh dokumentu:	article
ISSN:	1678-7064 0100-4042
DOI:	10.1590/S0100-40422013000800014
Popis:	A short and efficient synthesis of heptadeuterated 2,2,4,4,5,7,7-d7-cholestane (1) from cholesterol (3) is described. The deuterated material will be useful for the analysis of different sources of petroleum in analytical geochemistry laboratories as internal standard for quantification of steranes via gas chromatography-mass spectrometry (GC-MS).
Databáze:	Directory of Open Access Journals
Externí odkaz:	https://doaj.org/article/5f5274b26aa3480aae23a34710f55ed1 Zobrazit plný text záznamu View record in DOAJ