New spectral data of some flavonoids from Deguelia hatschbachii A.M.G. Azevedo

Autor: Magalhães Aderbal F., Tozzi Ana M. G. A., Magalhães Eva G., Moraes Valéria R. de S.
Jazyk: angličtina
Rok vydání: 2003
Předmět:
Zdroj: Journal of the Brazilian Chemical Society, Vol 14, Iss 1, Pp 133-137 (2003)
Druh dokumentu: article
ISSN: 0103-5053
Popis: From the roots of Deguelia hatschbachii, the known flavonoids scandenin (1), methyl robustate (2) and 4',5- dihydroxy-6-(3,3-dimethylalyll)-7-methoxy flavanone (3) were isolated and characterized by comparison of their spectroscopic data with those found in the literature. Now the inclusion of 1D- and 2D-NMR and MS/MS data has allowed the complete assignment of all hydrogen and carbon chemical shifts in their NMR spectra, as well as the elucidation of the fragmentation pathways of 1-3 in the mass spectrometer.
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