Synthesis and Characterization of Thermally-Reduced Graphene

Autor: Razieh Jabari seresht, Mohsen Jahanshahi, Ali Morad Rashidi, Ali Asghar Ghoreyshi
Jazyk: angličtina
Rok vydání: 2013
Předmět:
Zdroj: Iranica Journal of Energy and Environment, Vol 4, Iss 1, Pp 53-59 (2013)
Druh dokumentu: article
ISSN: 2079-2115
2079-2123
DOI: 10.5829/idosi.ijee.2013.04.01.09
Popis: Thermally-reduced graphene was obtained from reduction of graphene oxide (GO) via heat treatment under the hydrogen in the range of 300-1100°C. In order to find optimum tempreture, the synthesized graphene has been investigated by X-ray diffraction (XRD), FTIR spectroscopy as well as Raman spectroscopy. The result indicated that the reduced graphene at 900°C (GR900) had the highest quality in comparison with the other temperatures. Additionally, GR900 exhibited a sharp (002) peak corresponding to an interlayer distance of 3.39° A, which is close to that of conventional graphene (3.4°A). However, the structure of GR900 was also investigated by transmission electron microscopy (TEM), scanning electron microscopy (SEM) and the results supported the previous findings.
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