Synthesis of novel metal complexes of 5-(4-isopropoxyphenyl)-Nphenyl- 1,3,4-thiadiazol-2-amine
| Autor: | Ahmed AbdulAmier Hussain Al-Amiery, Muna A. Shakir, Maysoon Yousif |
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| Jazyk: | angličtina |
| Rok vydání: | 2009 |
| Předmět: | |
| Zdroj: | Engineering and Technology Journal, Vol 27, Iss 5, Pp 891-897 (2009) |
| Druh dokumentu: | article |
| ISSN: | 1681-6900 2412-0758 |
| DOI: | 10.30684/etj.27.5.4 |
| Popis: | New5-(4-isopropoxyphenyl)-N-phenyl-1,3,4-thiadiazol-2-amine have beensynthesized in good yield by the reaction of N-phenylhydrazinecarbothioamide with a 4-isopropoxybenzoic acid in phosphorusoxychloride. Cr(III), Co(II), Ni(II),Cu(II),Zn(II)and Cd(II) complexes of 5-(4-isopropoxyphenyl)-N-phenyl-1,3,4-thiadiazol-2-aminehave been prepared, and characterized by elemental analysis, FT-IR, and UV/visiblespectra moreover determination of molar ratio M:L , determination of metal content M%by flame atomic absorption spectroscopy, molar conductance in DMF. solution andmagnetic moments (μeff.). |
| Databáze: | Directory of Open Access Journals |
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