| Autor: |
Tingting Niu, Bin Zhou, Zehui Zhang, Xiujie Ji, Jianming Yang, Yuhan Xie, Hongqiang Wang, Ai Du |
| Jazyk: |
angličtina |
| Rok vydání: |
2020 |
| Předmět: |
|
| Zdroj: |
Nanomaterials, Vol 10, Iss 12, p 2527 (2020) |
| Druh dokumentu: |
article |
| ISSN: |
2079-4991 |
| DOI: |
10.3390/nano10122527 |
| Popis: |
Resorcinol-formaldehyde/titanium dioxide composite (RF/TiO2) gel was prepared simultaneously by acid catalysis and then dried to aerogel with supercritical fluid CO2. The carbon/titanium dioxide aerogel was obtained by carbonization and then converted to nanoporous titanium carbide/carbon composite aerogel via 800 °C magnesiothermic catalysis. Meanwhile, the evolution of the samples in different stages was characterized by X-ray diffraction (XRD), an energy-dispersive X-ray (EDX) spectrometer, a scanning electron microscope (SEM), a transmission electron microscope (TEM) and specific surface area analysis (BET). The results showed that the final product was nanoporous TiC/C composite aerogel with a low apparent density of 339.5 mg/cm3 and a high specific surface area of 459.5 m2/g. Comparing to C aerogel, it could also be considered as one type of highly potential material with efficient photothermal conversion. The idea of converting oxide–carbon composite into titanium carbide via the confining template and low-temperature magnesiothermic catalysis may provide new sight to the synthesis of novel nanoscale carbide materials. |
| Databáze: |
Directory of Open Access Journals |
| Externí odkaz: |
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