Mechanical-chemical synthesis Ba0.77Sr0.23TiO3

Autor: Kosanović D., Obradović N., Živojinović J., Filipović S., Maričić A., Pavlović V., Tang Y., Ristić M.M.
Jazyk: angličtina
Rok vydání: 2012
Předmět:
Zdroj: Science of Sintering, Vol 44, Iss 1, Pp 47-55 (2012)
Druh dokumentu: article
ISSN: 0350-820X
DOI: 10.2298/SOS1201047K
Popis: Barium-Strontium-Titanate Ba0.77Sr0.23TiO3 was prepared from starting materials BaCO3, SrCO3 and TiO2 through solid-state reactions. Mixtures of these oxides are mechanically activated in a high-energy planetary ball mill at different time intervals from 0 to 120 minutes. In order to obtain information on phase composition, crystal structure was determent by X-ray diffraction. It was observed that after 80 minutes in process synthesis Ba0.77Sr0.23TiO3 started Thermal analyzes were performed in order to determine the characteristic temperatures of the processes that occur in the solid phase. Particle size distribution, together with electron microscopy scanning has given us very useful information about the morphology of the powder.
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