| Autor: |
Jastrzębska Ilona, Szczerba Jacek, Stoch Paweł, Błachowski Artur, Ruebenbauer Krzysztof, Prorok Ryszard, Śnieżek Edyta |
| Jazyk: |
angličtina |
| Rok vydání: |
2015 |
| Předmět: |
|
| Zdroj: |
Nukleonika, Vol 60, Iss 1, Pp 47-49 (2015) |
| Druh dokumentu: |
article |
| ISSN: |
0029-5922 |
| DOI: |
10.1515/nuka-2015-0012 |
| Popis: |
In this work the synthesis of hercynite from Fe2O3 and Al2O3 powders was carried out by arc-melting method under the protective argon atmosphere. The obtained material was characterized with the use of powder X-ray diffractometry (XRD) and Mössbauer spectroscopy (MS). A Mössbauer effect in hercynite obtained by the arc-melting method indicated the cations distribution in the spinel structure among the tetrahedral and octahedral interstices. The presence of Fe2+ ions was detected in both tetrahedral and octahedral sites while Fe3+ ions occupied only the octahedral interstices. The approximate formula of the obtained iron-aluminate spinel was as follows (Fe2+0.77Al3+0.23) (Fe3+0.07Fe2+0.05Al0.88)2O4. |
| Databáze: |
Directory of Open Access Journals |
| Externí odkaz: |
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