Redetermination of catena-poly[[chloridolead(II)]-μ2-chlorido-di-μ2-thiourea-κ4S:S] at 100 K
| Autor: | Hafid Zouihri, Khalid Yamni, Youssef Messouss, Najib Tijani, Lahcen Messaoudi |
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| Jazyk: | angličtina |
| Rok vydání: | 2016 |
| Předmět: | |
| Zdroj: | IUCrData, Vol 1, Iss 11, p x161745 (2016) |
| Druh dokumentu: | article |
| ISSN: | 2414-3146 24143146 |
| DOI: | 10.1107/S2414314616017454 |
| Popis: | Although the structure rerefinement (CCD data at 100 K) of the polymeric lead(II) thiourea complex, [PbCl2·2tu]n where (tu = SCN2H4), basically confirmed the previous study based on integrated Weissenberg data recorded at room temperature [Nardelli & Fava (1959). Acta Cryst. 12, 727–732]; all atomic positions could be determined with significantly higher precision and accuracy. In addition, all H atoms could be located from difference maps, revealing details of the hydrogen-bonding scheme. |
| Databáze: | Directory of Open Access Journals |
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