Synthesis and research of polyfunctional silylureas used in electric deposition of tin-indium alloy

Autor: K. Yu. Ivanova, M. V. Kuzmin, L. G. Rogozhina, A. O. Patianova, V. L. Semenov, R. I. Alexandrov
Jazyk: angličtina
Rok vydání: 2021
Předmět:
Zdroj: Chimica Techno Acta, Vol 8, Iss 3 (2021)
Druh dokumentu: article
ISSN: 2411-1414
DOI: 10.15826/chimtech.2021.8.3.05
Popis: Polyfunctional silylureas were synthesized by the interaction of 3-aminopropyltriethoxysilane with isocyanates of various structures in an inert aromatic solvent. Commercially available diisocyanates such as isophorone diisocyanate, hexamethylene diisocyanate, 2,4-toluene diisocyanate were used as isocyanates. In this case, freshly distilled toluene was used as a solvent. The structures of the obtained compounds were confirmed by the data of IR and NMR1H spectroscopy. Using the synthesized compounds, formulations of compositions for electrodeposition of a tin-indium alloy on a copper wire were developed. The possibility of using silylureas of various structures as effective surfactants used in the electrodeposition of the tin-indium alloy is shown. The operational characteristics of the obtained wire were investigated, including the wire diameter, coating thickness, tensile strength, electrical resistance, and direct current electrical resistivity.
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