Synthesis And Characterization of 5-(Mercapto-1,3,4Thiadiazole-2yl)α,α-Diphenyl Methanol From Benzilic Acid
| Autor: | Muhanned J. Mahmoud, Redha I. AL-bayati, Shaimaa A. Saoud, Ismaeel Y. Majeed |
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| Jazyk: | angličtina |
| Rok vydání: | 2017 |
| Předmět: | |
| Zdroj: | Ibn Al-Haitham Journal for Pure and Applied Sciences, Vol 26, Iss 1 (2017) |
| Druh dokumentu: | article |
| ISSN: | 1609-4042 2521-3407 |
| Popis: | 5-(mercapto-1,3,4-thiadiazole-2yl)α,α-(diphenyl)methanol have been synthesized by ring closer of potassium xanthate[which have been prepared by reaction of benzilic acid hydrazide with carbon disulphide in potassium hydroxide] using conc.sulphuric acid at (0-5)°C scheme(I). Their characterization was carried out from T.L.C, M.P, FT.IR and 1H-NMR. |
| Databáze: | Directory of Open Access Journals |
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