Evaluation of uncertainty for the determination of thiocyanate in cheese by inhibited conductivity Ion Chromatography

Autor: PAN Can-sheng, ZHANG Zhi-zhou, XIA Bing, ZHANG Fei, WU Ping, WU Ling-tao
Jazyk: English<br />Chinese
Rok vydání: 2023
Předmět:
Zdroj: Shipin yu jixie, Vol 39, Iss 3, Pp 49-54,121 (2023)
Druh dokumentu: article
ISSN: 1003-5788
DOI: 10.13652/j.spjx.1003.5788.2022.80663
Popis: Objective: To evaluate the uncertainty of the determination of thiocyanate in cheese by inhibition conductance ion chromatography. Methods: The content of thiocyanate in cheese was determined by inhibition conductance ion chromatography and a mathematical model was established. The source of uncertainty introduced in the process of the experiment was described, and the synthetic uncertainty was calculated for each uncertainty component. Results: The determination of thiocyanate was (10.2±0.56) mg/kg, k=2, p=95%. Conclusion: The uncertainty in the measurement process mainly comes from the concentration of thiocyanate in the test solution, followed by sample recovery and repeatability experiments.
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