Determination of sodium and potassium in certified rock samples by AES after ultrasonic leaching

Autor: Özkan Hikmet Mehmet, Özkan Aysun, Gürkan Ramazan, Akçay Mehmed
Jazyk: angličtina
Rok vydání: 2006
Předmět:
Zdroj: Journal of the Serbian Chemical Society, Vol 71, Iss 8-9, Pp 949-955 (2006)
Druh dokumentu: article
ISSN: 0352-5139
1820-7421
DOI: 10.2298/JSC0609949O
Popis: In order to evaluate the data obtained by atomic emission spectrometric analysis after ultrasonic extraction, destructive analysis of some certified rock samples employing ultrasonic waves was applied to two elements, Na and K, and the recovery rates were defined. The recovery ratio as K1=CULM/CCRM was defined for the ultrasonic leaching method (CULM) and the certified reference materials (CRMs). Another recovery ratio, K 2 was also defined from the results of the conventional dissolution method (CCDM), that is K2 CULM/CCDM. The accuracy and precision of the method were comparable with those of the conventional methods. The obtained recoveries were between 90.0 %< K1, Na
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