FEW-LAYER GRAPHENE PARTICLES BASED ON THERMALLY EXPANDED COINTERCALATE OF GRAPHITE NITRATE WITH ACETIC AND FORMIC ACIDS

Autor: A.A. Davydova, E.V. Raksha, O.N. Oskolkova, V.V. Gnatovskaya, P.V. Sukhov, O.M. Padun, V.A. Glazunova, V.V. Burkhovetskij, G.K. Volkova, Yu.V. Berestneva, M.V. Savoskin
Jazyk: ruština
Rok vydání: 2020
Předmět:
Zdroj: Физико-химические аспекты изучения кластеров, наноструктур и наноматериалов, Iss 12, Pp 580-590 (2020)
Druh dokumentu: article
ISSN: 2226-4442
2658-4360
DOI: 10.26456/pcascnn/2020.12.580
Popis: Dispersions of graphene nanoparticles were obtained by liquid phase exfoliation of thermally expanded graphite in ethanol as well as tert-butanol via sonication. Initial thermally expanded graphite was obtained by heat treatment in the shock mode of ternary graphite nitrate intercalation compound with formic and acetic acids. Investigation of the graphite nitrate intercalation compound and thermally expanded graphite structural characteristics by X-ray diffraction analysis has been carried out. The microstructure and morphology of the obtained graphene particles were studied by transmission electron microscopy.
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