Simple synthesis of Black TiO 2 Nanofibers Via Calcination in Inert Atmosphere

Autor: Myeongjun Ji, Eung Ryong Kim, Mi-Jeong Park, Hee Yeon Jeon, Jaeyun Moon, Jongmin Byun, Young-In Lee
Jazyk: angličtina
Rok vydání: 2022
Předmět:
Zdroj: Archives of Metallurgy and Materials, Vol vol. 67, Iss No 4, Pp 1481-1486 (2022)
Druh dokumentu: article
ISSN: 2300-1909
DOI: 10.24425/amm.2022.141078
Popis: Black TiO 2nanofibers have recently emerged as a promising material that has both advantages of black metal oxide and one-dimensional nanostructure. However, current reduction-based synthesis approaches are not compatible with practical applications because these processes require high process costs, complicated processes, and sophisticated control. Therefore, it is still necessary to develop a simple and facile method that can easily introduce atomic defects during the synthesis process. This work suggests an electrospinning process with an antioxidant and subsequent calcination process for the facile synthesis of black TiO 2 nanofibers. The synthesized black TiO 2 nanofiber has an average diameter of 50.3 nm and a rutile structure. Moreover, this nanofiber represented a noticeable black color and a bandgap of 2.67 eV, clearly demonstrating the bandgap narrowing by the introduced atomic defects.
Databáze: Directory of Open Access Journals