Autor: |
Edward Lee, Richard A. Harris, Jacobus J. Terblans, Elizabeth Coetsee, Vinay Kumar, Hendrik C. Swart |
Jazyk: |
angličtina |
Rok vydání: |
2024 |
Předmět: |
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Zdroj: |
Chemical Physics Impact, Vol 9, Iss , Pp 100715- (2024) |
Druh dokumentu: |
article |
ISSN: |
2667-0224 |
DOI: |
10.1016/j.chphi.2024.100715 |
Popis: |
This study focuses on the synthesis of SrVO3 through the reduction of Sr2V2O7 by annealing in a reducing atmosphere. The effects of annealing temperature and annealing duration on Sr2V2O7 were investigated. The X-ray powder diffraction pattern showed that stoichiometric changes to Sr2V2O7 were achieved only at an elevated annealing temperature of 1000 °C in a reducing atmosphere, and that the desired SrVO3 was obtained only after 144 h of annealing. Further investigation of SrVO3 was performed using X-ray photoelectron spectroscopy, which confirmed that the reduction of V5+ found in Sr2V2O7 to V4+ found in SrVO3 was achieved. |
Databáze: |
Directory of Open Access Journals |
Externí odkaz: |
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