One-pot combustion synthesis of nickel oxide and hematite: From simple coordination compounds to high purity metal oxide nanoparticles
| Autor: | Jeremić Dejan, Anđelković Ljubica, Milenković Milica R., Šuljagić Marija, Šumar-Ristović Maja, Ostojić Sanja, Nikolić Aleksandar S., Vulić Predrag, Brčeski Ilija, Pavlović Vladimir |
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| Jazyk: | angličtina |
| Rok vydání: | 2020 |
| Předmět: | |
| Zdroj: | Science of Sintering, Vol 52, Iss 4, Pp 481-490 (2020) |
| Druh dokumentu: | article |
| ISSN: | 0350-820X 1820-7413 |
| DOI: | 10.2298/SOS2004481J |
| Popis: | This work is the first report of a very simple and fast one-pot synthesis of nickel oxide (NiO) and hematite (α-Fe2O3) nanoparticles by thermal decomposition of transition metal aqua complexes with camphor sulfonate anions. Obtained nanopowders were characterized by X-ray powder diffraction, Fourier transform IR analysis, scanning electron microscopy, and Energy-dispersive X-ray spectroscopy. X-ray powder diffraction confirmed the formation of high purity NiO and α-Fe2O3 crystal phases. In the case of α-Fe2O3, about five times larger average crystallite size was obtained. Fourier transform IR spectra of synthesized materials showed characteristic peaks for NiO and α-Fe2O3 nanostructures. To visualize the morphology and the chemical composition of the final products Scanning electron microscopy and Energy-dispersive X-ray spectroscopy were performed. The thermogravimetric analysis was done for a better understanding of the general thermal behavior of precursor compounds. This easy-to-perform and fast preparation method opens a broad range of obtained materials’ usage, particularly due to its economic viability |
| Databáze: | Directory of Open Access Journals |
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