Interface character distributions in WC/Co cemented carbide

Autor: YU Shunshi, CHEN Song, LI Guanghui, LI Hui, LIN Yan, LI Hongfeng, DAI Siyuan, WU Tizhen, WANG Weiguo
Jazyk: čínština
Rok vydání: 2024
Předmět:
Zdroj: Cailiao gongcheng, Vol 52, Iss 7, Pp 204-213 (2024)
Druh dokumentu: article
ISSN: 1001-4381
DOI: 10.11868/j.issn.1001-4381.2023.000110
Popis: Electron backscatter diffraction, five parameter analysis, overlap-pole-figure analysis and near coincident site analysis were used to investigate the interface character distributions of WC/WC grain boundaries and WC/Co phase boundaries in WC/Co cemented carbides under different heat treatment states. The results show that the WC/WC Σ2 grain boundaries with a fraction of 4.5% are generated in the oil-quenched sample after high temperature sintering. The fraction of Σ2 boundaries with interface matching features of {101¯0}/{101¯0} is 2.6%.The cobalt in this sample is basically face-centered-cubic structure, and the interface with the interface inter-connection features of {101¯0}WC/{001}Co,{101¯0}WC/{110}Co and {112¯0}WC/{110}Co is the main part of the WC/Co phase boundary. After tempering at 800 ℃, the samples with atmosphere protection and slow cooling in the furnace have the proportion and characteristics of WC/WC Σ2 grain boundaries, which are very close to those of oil-quenched samples.The cobalt in this sample is primarily hexagonal structure, and the interface with the interface inter-connection features of {101¯0}WC/{101¯0}Co and {112¯0}WC/{112¯0}Co is the main part of the WC/Co phase boundary.
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