A method for rapid microsynthesis of radioactive cholesterol esters

Autor: Karoly G. Pinter, James G. Hamilton, James E. Muldrey
Jazyk: angličtina
Rok vydání: 1964
Předmět:
Zdroj: Journal of Lipid Research, Vol 5, Iss 2, Pp 273-274 (1964)
Druh dokumentu: article
ISSN: 0022-2275
DOI: 10.1016/S0022-2275(20)40252-4
Popis: A simple method for synthesizing esters of labeled cholesterol of high specific activity is described. The formation of acyl chlorides takes 10 min and they are reacted with labeled cholesterol to form the cholesterol esters in another 5 min. Yields were 30–70% and radiopurities of 90–99.5% were achieved.
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