Autor: |
Łukasz Chrobak, Dorota Korte, Hanna Budasheva, Mirosław Maliński, Peter Rodič, Ingrid Milošev, Sylwia Janta-Lipińska |
Jazyk: |
angličtina |
Rok vydání: |
2022 |
Předmět: |
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Zdroj: |
Energies, Vol 15, Iss 11, p 4122 (2022) |
Druh dokumentu: |
article |
ISSN: |
1996-1073 |
DOI: |
10.3390/en15114122 |
Popis: |
This article presents the results of comparative investigations of thermal parameters of hybrid sol–gel coatings (named TMZ) prepared from tetraethyl orthosilicate and organically modified 3-methacryloxypropyltrimethoxysilane. The coatings were prepared with the addition of zirconium(IV) tetrapropoxide chelated with methacrylic acid. Two series of samples were investigated: the first series, TMZ-I, TMZ-II and TMZ-III, with different amounts of zirconium, and the second series, TMZ-I/Ce, TMZ-II/Ce and TMZ-III/Ce, with the addition of cerium nitrate. The influence of the amount of zirconium and cerium on the thermal parameters of the sol–gel coatings was next analyzed. Two non-destructive and photothermal techniques were used for this purpose: photothermal radiometry (PTR) and beam deflection spectroscopy (BDS). The thermal diffusivity and conductivity of the coatings were extracted from the frequency experiments and are presented and discussed. The two-layer model was applied to interpret the photothermal spectra. The results obtained using these two techniques are compared and discussed. |
Databáze: |
Directory of Open Access Journals |
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