Synthesis of Molybdenum Oxide Nanofibers with Multiple Surface Facets Via Electropsinning Followed by Rapid Thermal Treatment

Autor: Cheol-Hui Ryu, Young-In Lee
Jazyk: angličtina
Rok vydání: 2024
Předmět:
Zdroj: Archives of Metallurgy and Materials, Vol vol. 69, Iss No 2, Pp 493-496 (2024)
Druh dokumentu: article
ISSN: 2300-1909
DOI: 10.24425/amm.2024.149774
Popis: A MoO3 nanofiber prepared by electrospinning and subsequent heat treatment is attracting significant attention due to its structural advantages. Vibrant studies are being conducted to control its morphology and diameter to improve its properties. In this study, we demonstrated the synthesis of α-MoO3 nanofibers with multiple surface facets by controlling the heating rate and temperature in the heat treatment step for removing polymer and crystallizing MoO3 from the electrospun polymer/precursor nanofibers. The analysis results show that the faster heating rate and higher heat treatment temperature in the thermal treatment process are more favorable for forming a shape in which particles with facet planes are connected. Finally, we observed the morphological change according to the heat treatment time to confirm the effect of the heat treatment conditions on the shape of MoO3 and interpreted the results in terms of nucleation and crystal growth.
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