| Autor: |
Laura G Ceballos-Mendivil, Yannely Carvajal-Campos, Judith Tánori-Córdova, Jonathan C Luque-Ceballos, Heidi Villafán-Vidales, Claudio A Estrada |
| Jazyk: |
angličtina |
| Rok vydání: |
2020 |
| Předmět: |
|
| Zdroj: |
Materials Research Express, Vol 7, Iss 11, p 115014 (2020) |
| Druh dokumentu: |
article |
| ISSN: |
2053-1591 |
| DOI: |
10.1088/2053-1591/abcbb8 |
| Popis: |
The use of concentrated solar energy in processing ceramic materials is an attractive route to obtain these materials with low CO _2 emissions. In this work, nanostructures of monoclinic zirconia (m-ZrO _2 ) were obtained using concentrated solar energy provided by the IER-UNAM solar furnace as a heat source. In the first stage of the process, a Zr/O/C complex was obtained by sol-gel method at a temperature of 120 °C using zirconium n-propoxide and sorbitol as precursors reagents. This complex was used in a second stage to obtain m-ZrO _2 by heating it at a temperature of 1200 °C for one hour in air atmosphere. This last stage was performed in a solar furnace. Samples were analyzed by characterization techniques: FT-IR, TGA/DSC, XRD, TEM, and SEM confirming the formation of nanostructures of zirconia in monoclinic phase. |
| Databáze: |
Directory of Open Access Journals |
| Externí odkaz: |
|
