Xerogel p-anisidinapropilsílica: estudo da estabilidade térmica e da resistência à lixiviação com solventes p-anisidinepropylsilica xerogel: thermal stability and resistance to leaching by solvents

Autor: Leonardo Franken, Lisiane S. dos Santos, Elina B. Caramão, Tania M. H. Costa, Edilson V. Benvenutti
Jazyk: English<br />Spanish; Castilian<br />Portuguese
Rok vydání: 2002
Předmět:
Zdroj: Química Nova, Vol 25, Iss 4, Pp 563-566 (2002)
Druh dokumentu: article
ISSN: 0100-4042
1678-7064
DOI: 10.1590/S0100-40422002000400010
Popis: The xerogel p-anisidinepropylsilica was obtained. This solid presents some residual paraffin and also a small fraction of high organofunctionalized material that was leached in polar solvent. The xerogel purification could be achieved by exhaustively washing with hexane and dichloromethane solvents, or submitting the xerogel to thermal treatment up to 300 ºC, in vacuum. The resulting purified xerogel material present an appreciable thermal stability and resistance to leaching by solvents.
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