| Autor: |
Abdulla F. Alshater, Abbas S. Hakeem, Ablikim Bake, Hatim D. Mohamed, Hosni M. Ezuber, Alia Mustafa, Ruqayah R. Alnasser, Mezna K. Al Ruwaihi, Aysha I. Rashdan, Fatema A. Jaberi, Khadija S. Bahar |
| Jazyk: |
angličtina |
| Rok vydání: |
2024 |
| Předmět: |
|
| Zdroj: |
Crystals, Vol 14, Iss 8, p 692 (2024) |
| Druh dokumentu: |
article |
| ISSN: |
2073-4352 |
| DOI: |
10.3390/cryst14080692 |
| Popis: |
In a quest to vet UNS S32205 as a potential structural material to serve moderate-to-high temperature operations of NPP auxiliary components, the DL-EPR test was exploited. A bifronted scheme comprised of 650 and 850 °C discrete treatments intended to explore progressive eutectoid decomposition and degree-of-sensitization (DoS) scenarios was adopted. The nuance witnessed with yet another dual approach—the Cihal- and image processing (IP)-normalized signal landscape—was rationalized through its attribution to culprit microstructures. This was sought, inter alia, in the vicinity of grain boundaries and σ-phase inclusions by virtue of postmortem FESEM, STEM-EDX, HRTEM SAED and XRD ascertainment. Discernable reactivation-kinetics resurgence was believed to mark the onset of deleterious σ-phase dissolution. This only came into fruition with longer ageing times (8–17 h) at 650 °C and succumbed to prematurely (1 h), and at DC biases more cathodic than −0.25 VAg/AgCl with the 850 °C counterpart. Opportune corroboration was offered in ir/ia breakaway for the respective conditions, which was unveiled to be particularly pre-emptive (5 h) with IP- vs. Cihal-normalized peers (8 h) related to the 650 °C condition. Meanwhile, the 850 °C condition endured a similar surge after as little as 1 h of ageing across the board, which hints at concomitant sigma-phase culpability. |
| Databáze: |
Directory of Open Access Journals |
| Externí odkaz: |
|
