Oxide layer characterization by XRD and Rietveld refinements in maraging steel 300 aged in steam atmosphere

Autor: Vanessa Sanches Pereira da Silva, José Roberto Ferreira Neto, Silvia Lucas Ferreira da Silva, Diogo Costa de Oliveira, Fábio de Camargo
Jazyk: English<br />Portuguese
Rok vydání: 2021
Předmět:
Zdroj: Brazilian Journal of Radiation Sciences, Vol 9, Iss 1A (2021)
Druh dokumentu: article
ISSN: 2319-0612
DOI: 10.15392/bjrs.v9i1A.1573
Popis: Maraging steels are martensitic steels hardened by precipitation of intermetallic compounds in thermal aging, with good machining properties and high strength, fracture toughness and corrosion resistance, being used in aircraft parts and rocket motor-case, tooling applications and nuclear plants. During thermal aging in steam atmosphere a protective and corrosion resistant oxide layer is formed over the bulk. In this work, conventional Bragg-Brentano geometry was used to identify the phases formed in four specimens of maraging steel grade 300 with different surface finishes that were previously solution annealed twice at (950 ± 5) °C for 1 h, air-cooled, and submitted to oxidation process under positive pressure about 1.5 kPa of steam at (480 ± 5) °C for 6 h, followed by forced air-cooling. Diffraction patterns were measured employing CuKα radiation, ranging 20º
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