Powder Diffraction Data and Mesomorphic Properties for 4-Butyloxyphenyl 4'-Decyloxybenzoate

Autor: Cvetinov, M., Stojanović, M., Obadović, D., Rakić, S., Vajda, A., Fodor-Csorba, K., Éber, N.
Rok vydání: 2014
Předmět:
Zdroj: Russ. J. Phys. Chem. A, 88, 1142-1146, 2014
Druh dokumentu: Working Paper
DOI: 10.1134/S0036024414070115
Popis: Unit cell parameters obtained from X-ray powder diffraction data are presented for the crystalline phase of a liquid crystal 4-butyloxyphenyl 4'-decyloxybenzoate: a = 23.098 (4) {\AA}, b = 5.974 (6) {\AA}, c = 12.357 (10) {\AA}, \b{eta} = 121.53 (8){\deg}, unit-cell volume V = 1453.56 {\AA}3. Temperature dependent X-ray diffraction data confirmed the existence of smectic A and smectic C mesophases and a more ordered, tilted crystalline smectic phase. Possibility of existence of previously reported smectic B phase as well as another crystalline phase was refuted.
Databáze: arXiv