| Autor: |
Zhen-Fei, Zhang, Jia-Pei, Lü, Ying-Ying, Pei, Chun-Ying, Wang, Chang-Sheng, Guo, Jian, Xu |
| Rok vydání: |
2020 |
| Předmět: |
|
| Zdroj: |
Huan jing ke xue= Huanjing kexue. 41(3) |
| ISSN: |
0250-3301 |
| Popis: |
Organophosphate esters (OPEs) are ubiquitous in the environment and pose a potential threat to ecosystems and human health. A method for the determination of eight OPEs by ultra-performance liquid chromatography-tandem mass spectrometer (UPLC-MS/MS) was established. The recovery rates of eight target compounds with different solid-phase extraction columns, different eluents, and different eluent volumes were compared. The results showed that using ENVI-18 column enrichment, OPEs were eluted with 8 mL acetonitrile containing 25% (volume fraction) dichloromethane, and the labeled recovery rate of the target compound was 92.5%-102.2%. The recoveries of different matrix samples were 88.5%-116.1% and relative standard deviation was 1.7%-9.9%. The concentration range of 8 different detectable organophosphate esters in the effluent of sewage treatment plant is 85.9-235.4 ng·L |
| Databáze: |
OpenAIRE |
| Externí odkaz: |
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